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Creators/Authors contains: "Love, Robert"

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  1. ; ; ; ; ; ; (, Inorganic Chemistry)
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  2. ; ; ; (, Chemical Communications)
    null (Ed.)
    We report the synthesis of a cyclic hexavanadate polyoxovanadate-alkoxide cluster, [VO(OC2H5)2]6 , and its conversion, under solvothermal conditions, to an oxygen-deficient Lindqvist assembly, [V 6 O 6 (OC 2 H 5 ) 12 ] n ( n = 1−, 0). This study presents insights into the mechanism of organo-functionalized polyoxovandate-alkoxide formation, namely identifying essential intermediates and the source of the central μ 6 -O 2− ligand. 
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